Aug 14, 2024 · The following document provides information on the method to extract soluble cyanide salts and many insoluble cyanide complexes from wastes and leachates, designed to address the problem of "trace" analyses.

1.1 This method is a reflux-distillation procedure used to extract soluble cyanide salts and many insoluble cyanide complexes from wastes and leachates. It is based on the decomposition of nearly all cyanides by a reflux distillation procedure using a strong acid and a magnesium catalyst.

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This method provides a 3-step process to extract and measure cyanide in wastes and leachates: 1. Cyanide salts and complexes are decomposed through a reflux distillation procedure using acid and magnesium catalyst, releasing hydrocyanic acid (HCN). 2. The HCN is purged from the sample and absorbed in an alkaline scrubber solution. 3.

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